Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis
Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis
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Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis

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What is ISO 10810 - X-ray photoelectron spectroscopy about? 

ISO 10810 is applicable to X-ray photoelectron spectroscopy. It provides guidelines for analysing surface chemicals. 

ISO 10810 is intended to aid the operators of X-ray photoelectron spectrometers in their analysis of typical samples. It takes the operator through the analysis from the handling of the sample and the calibration and setting-up of the spectrometer to the acquisition of wide and narrow scans and also gives advice on quantification and on the preparation of the final report. 

Who is ISO 10810 - X-ray photoelectron spectroscopy for?  

ISO 10810 on X-ray photoelectron spectroscopy is useful for: 

  • X-ray laboratories 
  • Chemical industries 
  • Suppliers of XPS instruments 
  • Manufacturers of spectrometer devices 

Why should you use ISO 10810 - X-ray photoelectron spectroscopy 

X-ray photoelectron spectroscopy (XPS) is used extensively for the surface (1 nm to 10 nm) analysis of materials. 

ISO 10810 provides you with the guidance that will help you to identify, compare and measure XPS binding energies of their core levels with tabulations of those energies for the different elements. ISO 10810 helps you to determine chemical states from shifts in peak positions and other parameters compared with the data for that element in its pure elemental state. 

Information on the quantities of such elements can be derived from the measured intensities of photoelectron peaks. ISO 10810 sets out the calculation of the quantities of the constituent chemical species present in the surface layer studied (outer 1 nm to 10 nm) using formulae. 

Overall, ISO 10810 guides you with X-ray photoelectron spectrometers analysis of the surfaces (outer 1 nm to 10 nm) of typical samples. 

What’s changed since the last update? 

BS ISO 10810:2019 supersedes BS ISO 10810:2010, which is withdrawn. 

The main changes to the previous edition are as follows: 

  • Table 3: semiconductor wafer added as a specimen form 
  • 6.2.7: paragraph replaced to reflect modern practice 
  • 6.3.10: nanoparticles added as a material type 
  • Clause 8 and the flow chart in Figure 6 have been thoroughly revised to improve clarity. The cells in the flow chart now contain references to the appropriate subclause within Clause 8 
  • 8.2.1: it is now pointed out that the use of the C 1s peak provides only an approximate binding energy reference 
  • 9.3.3.3: mention has been made of the use of ionised clusters of inert gas atoms for depth profiling