1 Scope
This part of ISO 6721 describes a flexural, non-resonance method for determining the components of the
Young’s complex modulus E* of polymers at frequencies typically in the range 0,01 Hz to 100 Hz. Higher-frequency measurements can be made, but significant errors may be obtained
in the dynamic properties measured (see 10.2.1 and 10.2.2). The method is suitable for measuring dynamic storage moduli in the range 10 MPa to
200 GPa. Although materials with moduli less than 10 MPa may be studied, more accurate
measurements of their dynamic properties can be made using shear modes of deformation
(see part 6 of ISO 6721).
This method is particularly suited to the measurement of loss factors greater than
0,1 and may therefore be conveniently used to study the variation of dynamic properties
with temperature and frequency through most of the glass-rubber relaxation region
(see ISO 6721‑1:1994, subclause 9.4). The availability of data determined over wide ranges of both frequency and temperature
enables master plots to be derived, using frequency/temperature shift procedures,
which present dynamic properties over an extended frequency range at different temperatures.